岛津GC-14C气相色谱 分流比怎么设定 岛津GC-14c 气相色谱使用操作程序，我是新手，刚到一个单...
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\u8f7d\u6c14\u6d41\u901f
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\u8fdb\u6837\u91cf\u548c\u8fdb\u6837\u901f\u5ea6
\u8fdb\u6837\u91cf\u4e00\u822c\u4e0d\u8d85\u8fc72\u03bcL\u3002\u8fdb\u6837\u91cf\u5927\u65f6\u5e94\u9009\u7528\u5bb9\u79ef\u5927\u7684\u886c\u7ba1\uff0c\u5426\u5219\u4f1a\u53d1\u751f\u6837\u54c1\u5012\u704c\u3002\u8fdb\u6837\u901f\u5ea6\u5219\u5e94\u5feb\u4e00\u4e9b\uff0c\u6700\u597d\u7528\u81ea\u52a8\u8fdb\u6837\u5668\u3002\u82e5\u91c7\u7528\u624b\u52a8\u8fdb\u6837\uff0c\u8fdb\u6837\u901f\u5ea6\u7684\u91cd\u73b0\u6027\u4f1a\u5f71\u54cd\u5206\u6790\u7ed3\u679c\u3002
\u4e0d\u5206\u6d41\u8fdb\u6837\u7684\u89c4\u5219
\u8bbe\u5b9a\u8fdb\u6837\u53e3\u6e29\u5ea6\u6bd4\u6837\u54c1\u7ec4\u5206\u4e2d\u6700\u9ad8\u6cb8\u70b9\u7684\u6e29\u5ea6\u9ad820\u2103\u4ee5\u4e0a\uff1b
\u5efa\u8bae\u53ef\u4ee5\u4f7f\u7528\u201c\u4e09\u660e\u6cbb\u201d\u6280\u672f\uff08\u5373\u6ce8\u5c04\u9488\u5148\u5438\u4e00\u6bb5\u6eb6\u5242\uff0c\u518d\u5f80\u4e0a\u62c9\u4e00\u6bb5\u7a7a\u6c14\uff0c\u7136\u540e\u624d\u662f\u5c06\u6837\u54c1\u5438\u5165\u6ce8\u5c04\u9488\uff09\u8fdb\u6837\uff0c\u5feb\u901f\u6ce8\u5165\u6837\u54c1\uff0c\u8ba9\u6ce8\u5c04\u5668\u505c\u5728\u8fdb\u6837\u53e3\u51e0\u79d2\u949f\u4ee5\u786e\u4fdd\u6837\u54c1\u5b8c\u5168\u6c14\u6c7d\u5316\uff1b
\u4e00\u822c\u5730\uff0c\u5f00\u59cb\u65f6\u67f1\u6e29\u7bb1\u6e29\u5ea6\u8bbe\u5b9a\u4e3a\u6bd4\u6eb6\u5242\u7684\u6cb8\u70b9\u4f4e20ºC\uff0c\u4fdd\u63011\u5206\u949f\uff0c\u7136\u540e\u518d\u6839\u636e\u6837\u54c1\u9700\u8981\u7a0b\u5e8f\u5347\u6e29\uff1b
\u8fdb\u6837\u65f6\u95f4\u4e3a0.5-1.0 min\u540e\uff0c\u8fdb\u6837\u53e3\u5207\u6362\u5230\u5206\u6d41\u6a21\u5f0f\uff0c\u8f7d\u6c14\u6d41\u91cf\u81f3\u5c11\u5e94\u8bbe\u4e3a50 mL/min\uff1b
\u786e\u4fdd\u9694\u57ab\u5439\u626b\u6253\u5f00\uff0c\u5e76\u8bbe\u4e3a3-5 mL/ min\u3002
\u8f6c\u8f7d\uff1a\u300a\u5206\u6790\u6d4b\u8bd5\u767e\u79d1\u7f51\u300b
GC-14C\u6c14\u76f8\u8272\u8c31\u4eea\u64cd\u4f5c\u89c4\u7a0b
1\u3001\u64cd\u4f5c\u524d\u7684\u51c6\u5907
1\uff09\u8272\u8c31\u67f1\u7684\u5b89\u88c5\uff1a
2\uff09\u6c14\u4f53\u6d41\u91cf\u7684\u8c03\u8282\uff1a
\u2460\u8f7d\u6c14\uff08N2\uff09\u5f00\u542f\u6c2e\u6c14\u94a2\u74f6\u9ad8\u538b\u9600\u524d\uff0c\u9996\u5148\u68c0\u67e5\u4f4e\u538b\u9600\u7684\u8c03\u8282\u6746\u5e94\u5904\u4e8e\u91ca\u653e\u72b6\u6001\uff0c\u6253\u5f00\u9ad8\u538b\u9600\uff0c\u7f13\u7f13\u65cb\u52a8\u4f4e\u538b\u9600\u7684\u8c03\u8282\u6746\uff0c\u8c03\u8282\u81f3\u7ea60.6MPa\uff0c\u7f13\u7f13\u5f00\u542f\u4e3b\u673a\u4e0a\u8f7d\u6c14\u8fdb\u53e3\u538b\u529b\u8868\uff08P\uff09\uff0c\u4f7f\u538b\u529b\u8868\u6307\u793a\u4e3a5 Kg/cm2\uff0c\u518d\u7f13\u6162\u5f00\u542f\u8f7d\u6c14\u6d41\u91cf\u8868\uff08M\uff09\uff0c\u8c03\u8282\u6c2e\u6c14\u6d41\u91cf\u81f3\u5b9e\u9645\u64cd\u4f5c\u91cf\u3002
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3\uff09\u68c0\u6f0f\uff1a\u7528\u7682\u6db2\u68c0\u67e5\u67f1\u53ca\u5404\u8fde\u63a5\u5904\u662f\u5426\u6f0f\u6c14\u3002
2\u3001\u4e3b\u673a\u64cd\u4f5c
1\uff09\u63a5\u901a\u7535\u6e90\uff0c\u5f00\u542f\u4e3b\u673a\u7535\u6e90\uff08\u53f3\u4e0b\u4fa7\uff09,\u6b64\u65f6CITP.XX \u663e\u793a\u51fa\u6765,\u540c\u65f6 POLARITY lor2 \u7684\u706f\u4eae, RANGE\u706f\u4eae\u3002
2\uff09\u6e29\u5ea6\u8bbe\u7f6e\u5982\u4e0b\uff1a
\u2460\u8bbe\u5b9a\u68c0\u6d4b\u5668\u6e29\u5ea6 DET.T 200 ENT \u663e\u793a: DETT 200
\u2461\u8bbe\u5b9a\u8fdb\u6837\u53e3\u6e29\u5ea6 180 ENT \u663e\u793a: INJT 180
\u2462\u8bbe\u5b9a\u67f1\u6e29COL INT TEMR 80 ENT \u663e\u793a: CITP 80
\u2463\u8bbe\u5b9a\u67f1\u6e29\u5ef6\u7eed\u65f6\u95f4 COL INTI TIME 1 ENT \u663e\u793a: CIYM 1.0
\u2464\u8bbe\u5b9a\u67f1\u7684\u5347\u6e29\u901f\u5ea6 COL PROG 10 ENT \u663e\u793a: CPRI 10.0
\u2465\u8bbe\u5b9a\u8272\u8c31\u67f1\u7684\u6700\u7ec8\u6e29\u5ea6COL FINAL TEMP 150 ENT \u663e\u793a:CFP1 150
\u2466\u8bbe\u5b9a\u6700\u7ec8\u6e29\u5ea6\u7684\u65f6\u95f4COL FINAL TIME 2 ENT\u663e\u793a:CFM12.0
\u6ce8:\u5982\u4e0d\u9700\u7a0b\u5e8f\u5347\u7a33\u53ea\u9700\u524d\u4e09\u90e8\u5206\u64cd\u4f5c, \u2463-\u2466\u4e3a\u7a0b\u5e8f\u5347\u7a33\u8bbe\u7f6e.
\u2467\u8bbe\u5b9aFID\u63a7\u5236\u6761\u4ef6
DET 1 ENT \u663e\u793aDIRG FID \u68c0\u6d4b\u5668\u4e2dRANGE 2\u706f\u4eae.\uff08DET 1 NON\u8868\u660eFID\u672a\u5b89\u88c5\u6216\u63a7\u5236\u5f00\u5173\u4f4d\u4e8eOFF\u3002\uff09
RANGE 2 ENT \u663e\u793a DIPL 1 INJ\uff081\uff09\u706f\u4eae\u3002
\u2468Monitor \uff0c\u64cd\u4f5c\u663e\u793a\u68c0\u6d4b\u5668\u6216\u67f1\u6e29
MONIT DET.T or MONIT COL \u663e\u793a:DETT. XX
CITP .XX \u672a\u6309\u52a0\u70ed\u5f00\u5173,\u4e0d\u663e\u793a\u52a0\u70ed,\u6309START\u3002
\u6ce8\uff1a\u6309\u4e0b\u4e0a\u8ff0\u952e\u540e\uff0c\u65e0\u7279\u6b8a\u539f\u56e0\u4e0d\u5f97\u6309ENTER\u3002DETT.25\u663e\u793a\u5ba4\u7a33\u3002
\u2469START? MONIT DET-T \u663e\u793aCITP.27 \u7531\u4e8e\u4eea\u5668\u5f00\u542f,\u663e\u793a\u9ad8\u4e8e\u5ba4\u6e29.
MONIT COL \u5f00\u542f\u52a0\u70ed\u5f00\u5173\u540e\u663e\u793a\u52a0\u70ed\u4e2d\u7684\u6e29\u5ea6. \u63a5\u901a\u52a0\u70ed\u5f00\u5173.
3\u3001 \u70b9\u706b \u9002\u5f53\u8c03\u5c0f\u7a7a\u6c14\u6d41\u91cf\uff08\u6ce8\u610f\uff1a\u8c03\u5c0f\u7a7a\u6c14\u6d41\u91cf\u53ef\u6309\u4e3b\u673a\u8868\u5934IGNITE\uff09\u3002\u9002\u5f53\u8c03\u5927\u6c22\u6c14\u6d41\u91cf\uff0c\u7acb\u5373\u7528\u70b9\u706b\u5668\u70b9\u706b\uff0c\u53ef\u542c\u5230\u201c\u6251\u201d\u58f0\uff0c\u4e3a\u786e\u8bc1\u5df2\u70b9\u7740\uff0c\u53ef\u7528\u4e00\u5757\u73bb\u7483\uff08\u6216\u955c\u7247\uff09\u7f6e\u4e8e\u68c0\u6d4b\u5668\u55b7\u53e3\u5904\uff0c\u5982\u73bb\u7247\u4e0a\u6709\u96fe\uff0c\u8868\u660e\u706b\u5df2\u70b9\u7740\uff0c\u7136\u540e\u5c06\u6c2e\u6c14\u3001\u7a7a\u6c14\u548c\u6c22\u6c14\u8c03\u8282\u5230\u9884\u7f6e\u7684\u4f4d\u7f6e\u3002
4\u3001 \u4eea\u5668\u68c0\u6d4b\u5668\u8f93\u51fa\u8fde\u63a5\u9002\u5f53\u7684\u8272\u8c31\u6570\u636e\u5904\u7406\u673a\u540e\u5f00\u542f\u6570\u636e\u5904\u7406\u673a\uff0c\u8bbe\u5b9a\u5404\u9879\u53c2\u6570\uff0c\u89c2\u5bdf\u57fa\u7ebf\u72b6\u6001\u3002\u57fa\u7ebf\u5e73\u7a33\u540e\u68c0\u67e5\u53c2\u6570\u8bbe\u5b9a\u662f\u5426\u5408\u9002\u3002
5\u3001\u8fdb\u6837 \u7528\u5fae\u91cf\u6ce8\u5c04\u5668\u8fdb\u6837\uff0c\u540c\u65f6\u542f\u52a8\u6570\u636e\u5904\u7406\u673a\u91c7\u96c6\u8272\u8c31\u4fe1\u53f7\u3002\u5206\u6790\u5b8c\u6bd5\u540e\u505c\u6b62\u91c7\u96c6\u6570\u636e\uff0c\u7ecf\u6570\u636e\u5904\u7406\u540e\u6253\u51fa\u62a5\u544a\u3002
\u670b\u53cb\u53ef\u4ee5\u5230\u884c\u4e1a\u5185\u4e13\u4e1a\u7684\u7f51\u7ad9\u8fdb\u884c\u4ea4\u6d41\u5b66\u4e60\uff01
\u5206\u6790\u6d4b\u8bd5\u767e\u79d1\u7f51\u8fd9\u5757\u505a\u5f97\u4e0d\u9519\uff0c\u6c14\u76f8\u3001\u6db2\u76f8\u3001\u8d28\u8c31\u3001\u5149\u8c31\u3001\u836f\u7269\u5206\u6790\u3001\u5316\u5b66\u5206\u6790\u3001\u98df\u54c1\u5206\u6790\u3002\u8fd9\u65b9\u9762\u7684\u4e13\u5bb6\u6bd4\u8f83\u591a\uff0c\u57fa\u672c\u4e0a\u95ee\u9898\u90fd\u80fd\u5f97\u5230\u89e3\u7b54\uff0c\u6709\u95ee\u9898\u53ef\u53bb\u90a3\u63d0\u95ee\uff0c\u7f51\u5740\u767e\u5ea6\u641c\u4e0b\u5c31\u6709\u3002
跟浓度大小有关系，顶空可以稍微小些，因为顶空本身就少，直接进样要大些。
仪器有分流口，用皂泡流量计测定流速，除以总的载气流量，！
朋友可以到行业内专业的网站进行交流学习！
分析测试百科网这块做得不错，气相、液相、质谱、光谱、药物分析、化学分析、食品分析。这方面的专家比较多，基本上问题都能得到解答，有问题可去那提问，网址百度搜下就有。
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