延胡索乙素对照品来源
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\u5982\u679c\u8981\u6c42\u9ad8\u4e00\u70b9\uff0c\u51c6\u786e\u79f0\u53d60.500g\uff0c100mL\u5b9a\u5bb9\uff0c\u53d610mL\u7a00\u91ca\u6210100mL\u3002\u79f01.000g\uff0c\u914d100mL\u53d65mL\u7a00\u91ca\u6210100\u4e5f\u884c\u3002
\u539f\u56e0\u592a\u591a\u4e86\uff0c\u65e0\u6cd5\u4e00\u8a00\u4ee5\u853d\u4e4b
\u53ef\u80fd\u7684\u539f\u56e0\uff1a
1.\u68c0\u6d4b\u6ce2\u957f\u4e0d\u5408\u9002\uff0c280nm\u662f\u5ef6\u80e1\u7d22\u4e59\u7d20\u6700\u9002\u68c0\u6d4b\u6ce2\u957f\u5417\uff1f
2.HPLC \u7684\u7cfb\u7edf\u95ee\u9898
a\u3002\u67f1\u5b50\u4e0d\u597d\uff0c\u91c7\u7528\u4e86\u4e0d\u5408\u9002\u7684\u67f1\u5b50\uff0c\u6bd4\u5982\u6b63\u76f8\u67f1\u548c\u53cd\u76f8\u67f1\u5c31\u662f\u5b8c\u5168\u4e0d\u540c\u7684\u3002\u5982\u679c\u4e24\u5cf0\u4e0d\u5b8c\u5168\u5206\u79bb\uff0c\u5c31\u5e94\u8be5\u6362\u7528\u66f4\u957f\u7684\u67f1\u5b50\uff0c\u6216\u5176\u4ed6\u7c7b\u578b\u6216\u54c1\u724c\u7684\u67f1\u5b50
b\u3002\u4e0d\u5408\u9002\u7684\u6d41\u52a8\u76f8 \u6d41\u52a8\u76f8\u53ef\u76f4\u63a5\u5f71\u54cd\u6837\u54c1\u7684\u5206\u79bb\uff0c\u63a8\u8350\u5148\u6362\u6d41\u52a8\u76f8\uff0c\u6bd4\u5982\u589e\u52a0\u5176\u4e2d\u7684\u6c34\u7684\u6bd4\u4f8b
c\u3002\u6d41\u901f \u7a0d\u7a0d\u964d\u4f4e\u6d41\u901f\u53ef\u6539\u5584\u5206\u79bb
d\u3002\u4e0d\u51fa\u5cf0 \u68c0\u6d4b\u5668\u7075\u654f\u5ea6\u592a\u4f4e\u5bfc\u81f4\u68c0\u6d4b\u4e0d\u51fa
采纳哦
绛旓細寤惰儭绱箼绱犲鐓у搧鏉ユ簮:缃傜矡绉戞鐗╁欢鑳＄储(Corydalis yanhusuo W.T.Wang)鐨勫共鐕ュ潡鑼锛屼紡鐢熺传鍫囧潡鑼庯紝灏忚姳榛勫爣鍏ㄨ崏锛屾繁灞辩传鍫囨牴锛岄槻宸辩妞嶇墿鍗庡崈閲戣棨鏍癸紝鎴戜笂鏈堝湪璐靛窞杩ぇ鍏徃璁簡涓夋敮锛 寤惰儭绱箼绱犲鐓у搧鍚噺99% 寤惰儭绱箼绱犲鐓у搧妫娴嬫柟娉旽PLC娴嬪畾 寤惰儭绱箼绱犲鐓у搧鐢ㄩ:涓浗鑽吀瑙勫畾鎿嶄綔. 寤惰儭绱箼绱犲鐓...
绛旓細[鎴愬垎鏉ユ簮] 缃傜矡绉戞鐗╁欢鑳＄储锛堝厓鑳★級Corydalis yanhusuo W.T. Wang 鍧楄寧锛屽緱娑堟棆浣擄紝浼忕敓绱爣C.decumbens锛圱hunb.锛塒er.S锛庡潡鑼庯紝寰楁秷鏃嬩紞锛屽皬鑺遍粍鍫 C.racemosa锛圱hunb锛庯級Pers.鍏ㄨ崏锛屽緱娑堟棆浣擄紝榛勮寯锛堟繁灞辩传鍫囷級C.pallida锛圱hunb锛庯級Pers. 鏍癸紝寰楁秷鏃嬩綋锛岄槻宸辩妞嶇墿鍗庡崈閲戣棨 Stephania sinica Diel...
绛旓細瀵圭収鍝佹恫锛氬彇寤惰儭绱箼绱犲鐓у搧锛屽姞涔欓唶鍒舵垚姣1ml鍚1mg鐨勬憾娑诧紝浣滀负瀵圭収鍝佹憾娑层傚睍寮锛2%姘㈡哀鍖栭挔姘存憾娑茬鑳禛钖勫眰鏉匡紝浠ユ宸辩兎锛嶆隘浠匡紞鐢查唶锛7锛5锛4锛1锛変负灞曞紑鍓傦紝灞曡窛8cm銆傛樉鑹诧細渚濇鍠风█纰樺寲閾嬮捑璇曟恫鍜屼簹纭濋吀閽犱箼閱囨憾娑诧紝鏃ュ厜涓嬫瑙嗭紝渚涜瘯鍝佽壊璋卞湪涓庡鐓у搧鑹茶氨鐩稿簲鐨勪綅缃笂鏄剧浉鍚岀殑妫曡壊鑹叉枒銆
绛旓細(2)鍙栨湰鍝佺矇鏈1g,鍔犵敳閱50ml,瓒呭０澶勭悊30鍒嗛挓,婊よ繃,婊ゆ恫钂稿共,娈嬫福鍔犳按10ml浣挎憾瑙,鍔犳祿姘ㄨ瘯娑茶皟鑷冲牽鎬,鐢ㄤ箼閱氭尟鎽囨彁鍙3娆,姣忔10ml,鍚堝苟涔欓啔娑,钂稿共,娈嬫福鍔犵敳閱1ml浣挎憾瑙,浣滀负渚涜瘯鍝佹憾娑层傚彟鍙寤惰儭绱㈠鐓鑽潗1g,鍚屾硶鍒舵垚瀵圭収鑽潗婧舵恫銆傚啀鍙寤惰儭绱箼绱犲鐓у搧,鍔犵敳閱囧埗鎴愭瘡1ml鍚0.5mg鐨勬憾娑,浣滀负瀵圭収鍝佹憾娑层傜収...
绛旓細10渭l銆2. 2. 2 渚涜瘯鍝佹憾娑茬殑鍒跺鍒嗗埆鍙栦互涓4绉嶆彁鍙栨恫鍚5 m,l缃50ml瀹归噺鐡朵腑,鍔犵敳閱囧畾瀹硅嚦鍒诲害,鎽囧寑,浠0. 45渭m鐨勫井瀛旀护鑶滄护杩,鍗冲緱銆2. 2. 3 鏍囧噯鏇茬嚎鐨勫埗澶囧彇寤惰儭绱箼绱犲鐓у搧閫傞噺,绮惧瘑绉板畾,缃簬10 ml鐨勫閲忕摱涓,浠ョ敳閱囨憾瑙ｅ苟绋閲婅嚦鍒诲害,寰楁祿搴︿负0. 48 mg/ml鐨勬爣鍑嗗偍澶囨恫,鍐嶅垎鍒...
绛旓細鍦ㄥ埗澶囦緵璇曞搧婧舵恫杩囩▼涓紝灏20g鏍峰搧缃簬閿ュ舰鐡朵腑锛屽姞鍏80%涔欓唶骞惰秴澹板鐞嗭紝杩囨护鍚庤捀骞诧紝娈嬫福鐢ㄤ箼閱囨憾瑙ｏ紝缁忔皑璇曟恫璋冭妭纰辨э紝涔欓啔鎻愬彇涓ゆ鍚庡悎骞讹紝鍐嶇敤钖勫眰鑹茶氨娉曡繘琛屽垎鏋愶紝缁撴灉鏄剧ず涓寤惰儭绱箼绱犲鐓у搧鏈夌浉鍚岀殑棰滆壊鏂戠偣锛岀鍚堟爣鍑嗐傚湪绮掑害妫娴嬩腑锛屽5琚嬫牱鍝佽繘琛岃繃绛涳紝瑕佹眰涓嶈兘閫氳繃浜屽彿绛涘拰鑳介氳繃涔濆彿绛涚殑...
绛旓細鍙﹀彇寤惰儭绱㈠鐓鑽潗1g,鍚屾硶鍒舵垚瀵圭収鑽潗婧舵恫銆傚啀鍙寤惰儭绱箼绱犲鐓у搧锛屽姞鐢查唶鍒舵垚姣1ml鍚1mg鐨勬憾娑诧紝浣滀负瀵圭収鍝佹憾娑层傜収钖勫眰鑹茶氨娉曪紙闄勫綍鈪 B锛夎瘯楠岋紝鍚稿彇涓婅堪涓夌婧舵恫鍚2锝3渭l,鍒嗗埆鐐逛簬鍚屼竴鐢1锛呮阿姘у寲閽犲埗澶囩殑纭呰兌G钖勫眰鏉夸笂锛屼互姝ｅ繁鐑凤紞姘豢锛嶇敳閱囷紙7.5:4:1锛 涓哄睍寮鍓傦紝缃互灞曞紑鍓傞楗卞拰鐨...
绛旓細瀵逛簬寤惰儭绱㈤儴鍒嗭紝鍙3g鏈搧锛屽姞鍏80锛呬箼閱囧洖娴30鍒嗛挓锛岃繃婊ゅ苟娴撶缉锛屾畫娓ｇ敤姘ㄨ瘯娑茶皟鑷崇⒈鎬э紝鍐嶇敤涔欓啔鎻愬彇骞跺共鐕ャ傚鐓ц嵂鏉愬欢鑳＄储鍜寤惰儭绱箼绱犲鐓у搧鍒嗗埆鍒跺婧舵恫锛岃繘琛屽悓鏍风殑钖勫眰鑹茶氨娉曟娴嬶紝缁撴灉鏄剧ず渚涜瘯鍝佽壊璋卞湪瀵圭収鑽潗鍜屽鐓у搧浣嶇疆鏄剧ず鐩稿悓鐨勮崸鍏夋枒鐐广傛渶鍚庯紝鏁翠釜杩囩▼闇绗﹀悎涓稿墏涓浗鑽吀1995骞翠竴閮ㄩ檮褰曗厾 A...
绛旓細鎺ヤ笅鏉ワ紝灏嗘湰鍝佽皟鏁磒H鑷11锝10锛岀敤姘豢鎻愬彇鍚庯紝娈嬫福鍔犲叆涔欓唶婧惰В锛岃繘琛岀浜屾钖勫眰鑹茶氨娉曡瘯楠屻備互寤惰儭绱㈠鐓鑽潗鍜寤惰儭绱箼绱犲鐓у搧涓哄弬鐓э紝鐐规牱鍦1%姘㈡哀鍖栭挔婧舵恫璋冨埗鐨勭鑳禛鏉夸笂锛屽睍寮鍚庡湪纰樿捀姘斿拰绱鍏夌伅涓嬭瀵燂紝渚涜瘯鍝佸湪鐩稿簲浣嶇疆鏄剧浉鍚岄鑹茬殑鏂戠偣鎴栬崸鍏夋枒鐐癸紝杩涗竴姝ョ‘璁や簡鍏舵垚鍒嗙殑鍖归厤鎬с傛渶鍚庯紝浠...
绛旓細鍙栨湰鍝0.2g銆傚姞姘20ml銆備笌绋纭吀鍛堝井閰告у緟婧惰В鍚庣収涓嬭堪鏂规硶璇曢獙锛氣憼鍙栨憾娑2ml銆傚姞1%涓夋隘閱嬮吀锛屽嵆鐢熸垚鐧借壊娌夋穩銆傗憽鍙栨憾娑2ml.鍔犻噸缁滈吀閽捐瘯娑2婊淬傚嵆鐢熸垚榛勮壊娌夋穩銆傗憿鍙栨憾娑2ml锛屽姞1%閾佹阿鍖栭捑0.4ml銆備笌1%涓夋隘鍖栭搧璇曟恫0.3ml鐨勬贩鍚堟恫銆傚嵆鏄炬繁缁胯壊娓愬彉娣辫摑鑹层
